Staff information

Jian Hu

Catalysis Characterization
Chemist
Pacific Northwest National Laboratory
PO Box 999
MSIN: J7-10
Richland, WA 99352
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Biography

Dr. Jian Zhi Hu is a senior scientist (Level-V) at Pacific Northwest National Laboratory (PNNL) and is a mentor for junior scientist, postdoctor and graduate student research. Dr. Hu joined PNNL in 2000. Prior to then, Dr. Hu was an assistant research professor at University of Utah's Department of Chemistry from 2000 to 2001; and a research professor and associate at several scientific institutions.

Dr. Hu has nearly 30 year's research experience in solid state and liquid state nuclear magnetic resonance (NMR), magnetic resonance spectroscopy (MRS) and imaging (MRI). Dr. Hu has developed, including pioneering, many techniques, including:

Slow and ultra slow magic angle spinning, or magic angle turning (MAT) NMR techniques with sample spinning rate ranged from 1 to about 1000 Hz for enhanced spectral resolution in solids, semi-solids and biological materials
The combined high temperature (up to 240 C or more) and high pressure (up to 50 atm or more) MAS NMR
Constant flow MAS NMR for in situ characterization of heterogeneous catalyst materials and reaction mechanisms
in situ NMR capabilities for energy storage systems such as Li-ion, Li-S, Li-metal and non-aqueous flow batteries
High-resolution proton NMR metabolic profiling in vitro in human body fluids, ex vivo in excised intact tissues/organs, and in vivo in live animals
High-resolution and -sensitivity proton metabolite NMR spectrum on samples with very limited masses and volumes.

Dr. Hu is an author and co-author of about 147 peer-reviewed publications. He holds 6 issued U.S. patents, 3 foreign patents and one R&D 100 award that are all related to NMR technology development and applications.

Research Interests

Developing unique high resolution slow-MAS NMR metabolomics for biosignature discovery in biological tissues with sample volume from less than about 0.2 microliter to more than 1 cubic centimeter using a single probe;
In situ and ex situ NMR characterization of heterogeneous solid catalyst materials, surface functional groups and active cites, molecular dynamics at the interface, reaction mechanisms and pathways;
In situ constant flow and high pressure MAS NMR capability development;
In situ NMR capability development and applications for energy storage systems such as Li-ion, Li-S, Li-Air and non-aqueous flow batteries;
Ultra-high field NMR spectroscopy, quantum chemistry calculations to predict molecular geometry and the principal values of chemical shift tensors, and quadrupolar coupling constants; and NMR lineshape simulation, NMR pulse sequence design, programming, and testing.

Education and Credentials

Ph.D., Applied Physics, Wuhan Institute of Physics, Chinese Academy of Sciences
M.S., Applied Physics, Wuhan Institute of Physics, Chinese Academy of Sciences
B.S., Physics, Lanzhou University, China

Affiliations and Professional Service

ACS member

Awards and Recognitions

Special Academic President Award of the Chinese Academy of Sciences in 1995.
2012 R&D100 Award on graphene based materials for lithium ion battery application.

PNNL Publications

2023

Zhang W., S. Kim, L. Wahl, R. Khare, L.V. Hale, J.Z. Hu, and D.M. Camaioni, et al. 2023. "Low-temperature upcycling of polyolefins into liquid alkanes via tandem cracking-alkylation." Science 379, no. 6634:807-811. PNNL-SA-179736. doi:10.1126/science.ade7485

2022

Hu J.Z., N.R. Jaegers, N.T. Hahn, W. Hu, K. Han, Y. Chen, and J.A. Sears, et al. 2022. "Understanding the Solvation-Dependent Properties of Cyclic Ether Multivalent Electrolytes Using High Field NMR and Quantum Chemistry." JACS Au 2, no. 4:917-932. PNNL-SA-165254. doi:10.1021/jacsau.2c00046

2021

Han K., N.T. Hahn, K.R. Zavadil, N.R. Jaegers, Y. Chen, J.Z. Hu, and V. Murugesan, et al. 2021. "Factors Influencing Preferential Anion Interactions during Solvation of Multivalent Cations in Ethereal Solvents." Journal of Physical Chemistry C 125, no. 11:6005-6012. PNNL-SA-156316. doi:10.1021/acs.jpcc.0c09830
Jaegers N.R., W. Hu, T.J. Weber, and J.Z. Hu. 2021. "Low temperature (<200°C) degradation of electronic nicotine delivery system liquids generates toxic aldehydes." Scientific Reports 11, no. 1:Article No. 7800. PNNL-SA-153706. doi:10.1038/s41598-021-87044-x
Jaegers N.R., Y. Wang, J.Z. Hu, and I. Wachs. 2021. "Impact of Hydration on Supported V2O5/TiO2 Catalysts as Explored by Magnetic Resonance Spectroscopy." Journal of Physical Chemistry C 125, no. 30:16766-16775. PNNL-SA-157476. doi:10.1021/acs.jpcc.1c04150
Khivantsev K., N.R. Jaegers, L. Kovarik, M. Wang, J.Z. Hu, Y. Wang, and M.A. Derewinski, et al. 2021. "The Superior Hydrothermal Stability of Pd/SSZ-39 in Low Temperature Passive NOx Adsorption (PNA) and Methane Combustion." Applied Catalysis B: Environmental 280. PNNL-SA-151139. doi:10.1016/j.apcatb.2020.119449
Lai J., N.R. Jaegers, B. Mosevitzky Lis, M. Guo, M.E. Ford, E.D. Walter, and Y. Wang, et al. 2021. "Structure-Activity Relationships of Hydrothermally Aged Titania-Supported Vanadium-Tungsten Oxide Catalysts for SCR of NOx Emissions with NH3." ACS Catalysis 11, no. 19:12096-12111. PNNL-SA-158279. doi:10.1021/acscatal.1c02130
Lee I., M. Lee, L. Tao, T. Ikuno, R. Khare, A. Jentys, and T. Huthwelker, et al. 2021. "Activity of Cu-Al-oxo extra-framework clusters for selective methane oxidation on Cu exchanged zeolites." JACS Au 1, no. 9:1412-1421. PNNL-SA-160856. doi:10.1021/jacsau.1c00196
Li H., D. Guo, N.Z. Ulumuddin, N.R. Jaegers, J. Sun, B. Peng, and J. McEwen, et al. 2021. "Elucidating the Cooperative Roles of Water and Lewis Acid-Base Pairs in Cascade C-C Coupling and Self-Deoxygenation Reactions." JACS Au 1, no. 9:1471-1487. PNNL-SA-164561. doi:10.1021/jacsau.1c00218

2020

Chen Y., N.R. Jaegers, H. Wang, K. Han, J.Z. Hu, K.T. Mueller, and V. Murugesan. 2020. "Role of Solvent Rearrangement on Mg2+ Solvation Structures in Dimethoxyethane Solutions Using Multimodal NMR Analysis." The Journal of Physical Chemistry Letters 11, no. 15:6443-6449. PNNL-SA-153110. doi:10.1021/acs.jpclett.0c01447
Dagle V., A.D. Winkelman, N.R. Jaegers, J. Saavedra Lopez, J.Z. Hu, M.H. Engelhard, and S. Habas, et al. 2020. "Single-Step Conversion of Ethanol to n-Butene over Ag-ZrO2/SiO2 Catalysts." ACS Catalysis 10, no. 18:10602-10613. PNNL-SA-151691. doi:10.1021/acscatal.0c02235
Graham T.R., M. Dembowski, J.Z. Hu, N.R. Jaegers, X. Zhang, S.B. Clark, and C.I. Pearce, et al. 2020. "Intermediate Species in the Crystallization of Sodium Aluminate Hydroxy Hydrates." Journal of Physical Chemistry C 124, no. 23:12337-12345. PNNL-SA-150266. doi:10.1021/acs.jpcc.0c00205
Han K., Z. Yu, H. Wang, P.C. Redfern, L. Ma, L. Cheng, and Y. Chen, et al. 2020. "Origin of Unusual Acidity and Li+ Diffusivity in a Series of Water-in-Salt Electrolytes." Journal of Physical Chemistry B 124, no. 25:5284-5291. PNNL-SA-151945. doi:10.1021/acs.jpcb.0c02483
Jaegers N.R., K.T. Mueller, Y. Wang, and J.Z. Hu. 2020. "Variable Temperature and Pressure Operando MAS NMR for Catalysis Science and Related Materials." Accounts of Chemical Research 53, no. 3:611-619. PNNL-SA-148734. doi:10.1021/acs.accounts.9b00557
Jaegers N.R., W. Hu, Y. Wang, and J.Z. Hu. 2020. "High-Temperature and High-Pressure In Situ Magic Angle Spinning Nuclear Magnetic Resonance Spectroscopy." Journal of Visualized Experiments (JoVE). PNNL-SA-153912. doi:10.3791/61794
Jaegers N.R., Y. Wang, and J.Z. Hu. 2020. "Thermal perturbation of NMR properties in small polar and non-polar molecules." Scientific Reports 10, no. 1:Article No. 6097. PNNL-SA-148427. doi:10.1038/s41598-020-63174-6
Khivantsev K., N.R. Jaegers, L. Kovarik, J.Z. Hu, F. Gao, Y. Wang, and J. Szanyi. 2020. "Palladium/Zeolite Low Temperature Passive NOx Adsorbers (PNA): Structure-Adsorption Property Relationships for Hydrothermally Aged PNA Materials." Emission Control Science and Technology 6. PNNL-SA-141069. doi:10.1007/s40825-019-00139-w
Li H., J. Pang, N.R. Jaegers, L. Kovarik, M.H. Engelhard, A.W. Savoy, and J.Z. Hu, et al. 2020. "Conversion of ethanol to 1,3-butadiene over Ag-ZrO2/SiO2 catalysts: The role of surface interfaces." Journal of Energy Chemistry 54. PNNL-SA-153728. doi:10.1016/j.jechem.2020.05.038

2019

Graham T.R., J.Z. Hu, X. Zhang, M. Dembowski, N.R. Jaegers, C. Wan, and M.E. Bowden, et al. 2019. "Unraveling Gibbsite Transformation Pathways into LiAl-LDH in Concentrated Lithium Hydroxide." Inorganic Chemistry 58, no. 18:12385-12394. PNNL-SA-138626. doi:10.1021/acs.inorgchem.9b02000
Hu J.Z., N.R. Jaegers, Y. Chen, K. Han, H. Wang, V. Murugesan, and K.T. Mueller. 2019. "Adsorption and thermal decomposition of electolytes on nanometer magnesium oxide: An in situ 13C MAS NMR study." ACS Applied Materials & Interfaces 11, no. 42:38689-38696. PNNL-SA-144709. doi:10.1021/acsami.9b11888
Jaegers N.R., J. Lai, Y. He, E.D. Walter, D.A. Dixon, M. Vasiliu, and Y. Chen, et al. 2019. "Mechanism by which Tungsten Oxide Promotes the Activity of Supported V2O5/TiO2 Catalysts for NOX Abatement: Structural Effects Revealed by 51V MAS NMR Spectroscopy." Angewandte Chemie International Edition 58, no. 36:12609-12616. PNNL-SA-141251. doi:10.1002/anie.201904503
Jaegers N.R., K. Khivantsev, L. Kovarik, D.W. Klas, J.Z. Hu, Y. Wang, and J. Szanyi. 2019. "Catalytic activation of ethylene C-H bonds on uniform d8 Ir(I) and Ni(II) cations in zeolites: toward molecular level understanding of ethylene polymerization on heterogeneous catalysts." Catalysis Science & Technology 9, no. 23:6570-6576. PNNL-SA-148436. doi:10.1039/C9CY01442J
Wang M., N.R. Jaegers, M. Lee, C. Wan, J.Z. Hu, H. Shi, and D. Mei, et al. 2019. "Genesis and Stability of Hydronium Ions in Zeolite Channels." Journal of the American Chemical Society 141, no. 8:3444-3455. PNNL-SA-136963. doi:10.1021/jacs.8b07969
Zhang X., W. Cui, J.Z. Hu, H. Wang, M.P. Prange, C. Wan, and N.R. Jaegers, et al. 2019. "Transformation of Gibbsite to Boehmite in Caustic Aqueous Solution at Hydrothermal Conditions." Crystal Growth & Design 19, no. 10:5557-5567. PNNL-SA-146423. doi:10.1021/acs.cgd.9b00468
Zhang Y., R. Zhao, M. Sanchez-Sanchez, G.L. Haller, J.Z. Hu, R. Bermejo-Deval, and Y. Liu, et al. 2019. "Promotion of protolytic pentane conversion on H-MFI zeolite by proximity of extra-framework aluminum oxide and Br�nsted acid sites." Journal of Catalysis 370. PNNL-SA-154782. doi:10.1016/j.jcat.2019.01.006

2018

Graham T.R., K. Han, M. Dembowski, A. Krzysko, X. Zhang, J.Z. Hu, and S.B. Clark, et al. 2018. "27Al Pulsed Field Gradient, Diffusion-NMR Spectroscopy of Solvation Dynamics and Ion Pairing in Alkaline Aluminate Solutions." Journal of Physical Chemistry B 122, no. 48:10907-10912. PNNL-SA-138291. doi:10.1021/acs.jpcb.8b10145
Graham T.R., M. Dembowski, E. Martinez Baez, X. Zhang, N.R. Jaegers, J.Z. Hu, and M.S. Gruszkiewicz, et al. 2018. "In-Situ 27Al NMR Spectroscopy of Aluminate in Sodium Hydroxide Solutions Above and Below Saturation with Respect to Gibbsite." Inorganic Chemistry 57, no. 19:11864-11873. PNNL-SA-132754. doi:10.1021/acs.inorgchem.8b00617
Hu J.Z., N. Rajput, C. Wan, Y. Shao, X. Deng, N.R. Jaegers, and M.Y. Hu, et al. 2018. "25Mg NMR and Computational Modeling Studies of the Solvation Structures and Molecular Dynamics in Magnesium Based Liquid Electrolytes." Nano Energy 46. PNNL-SA-130126. doi:10.1016/j.nanoen.2018.01.051
Hu J.Z., N.R. Jaegers, M.Y. Hu, and K.T. Mueller. 2018. "In Situ and Ex Situ NMR for Battery Research." Journal of Physics: Condensed Matter 30, no. 46:Article No. 463001. PNNL-SA-134425. doi:10.1088/1361-648X/aae5b8
Prodinger S., A. Vjunov, J.Z. Hu, J.L. Fulton, D.M. Camaioni, M.A. Derewinski, and J.A. Lercher. 2018. "Elementary Steps of Faujasite Formation Followed by in situ Spectroscopy." Chemistry of Materials 30, no. 3:888-897. PNNL-SA-130041. doi:10.1021/acs.chemmater.7b04554
Shi D., H. Wang, L. Kovarik, F. Gao, C. Wan, J.Z. Hu, and Y. Wang. 2018. "WOx supported on gamma-Al2O3 with different morphologies as model catalysts for alkanol dehydration." Journal of Catalysis 363. PNNL-SA-132764. doi:10.1016/j.jcat.2018.04.004
Xue N., A. Vjunov, S. Schallmoser, J.L. Fulton, M. Sanchez-Sanchez, J.Z. Hu, and D. Mei, et al. 2018. "Hydrolysis of zeolite framework aluminum and its impact on acid catalyzed alkane reactions." Journal of Catalysis 365. PNNL-SA-139124. doi:10.1016/j.jcat.2018.07.015
Zhang X., P.I. Huestis, C.I. Pearce, J.Z. Hu, K. Page, L.M. Anovitz, and A. Aleksandrov, et al. 2018. "Boehmite and Gibbsite Nanoplates for the Synthesis of Advanced Alumina Products." ACS Applied Nano Materials 1, no. 12:7115-7128. PNNL-SA-139693. doi:10.1021/acsanm.8b01969

2017

Chen J., W.A. Henderson, H. Pan, B.R. Perdue, R. Cao, J.Z. Hu, and C. Wan, et al. 2017. "Improving Lithium-sulfur Battery Performance under Lean Electrolyte through Nanoscale Confinement in Soft Swellable Gels." Nano Letters 17, no. 5:3061-3067. PNNL-SA-121812. doi:10.1021/acs.nanolett.7b00417
Hu J.Z., C. Wan, A. Vjunov, M. Wang, Z. Zhao, M.Y. Hu, and D.M. Camaioni, et al. 2017. "27Al MAS NMR Studies of HBEA Zeolite at Low to High Magnetic Fields." Journal of Physical Chemistry C 121, no. 23:12849-12854. PNNL-SA-125685. doi:10.1021/acs.jpcc.7b03517
Hu J.Z., X. Zhang, N.R. Jaegers, C. Wan, T.R. Graham, M.Y. Hu, and C.I. Pearce, et al. 2017. "Transitions in Al Coordination During Gibbsite Crystallization Using High-Field 27Al and 23Na MAS NMR Spectroscopy." Journal of Physical Chemistry C 121, no. 49:27555-27565. PNNL-SA-130259. doi:10.1021/acs.jpcc.7b10424
Jaegers N.R., C. Wan, M.Y. Hu, M. Vasiliu, D.A. Dixon, E.D. Walter, and I. Wachs, et al. 2017. "Investigation of silica-supported vanadium oxide catalysts by high-field 51V Magic Angle Spinning NMR." Journal of Physical Chemistry C 121, no. 11:6246-6254. PNNL-SA-124184. doi:10.1021/acs.jpcc.7b01658
Prodinger S., H. Shi, S. Eckstein, J.Z. Hu, M.V. Olarte, D.M. Camaioni, and M.A. Derewinski, et al. 2017. "Stability of Zeolites in Aqueous Phase Reactions." Chemistry of Materials 29, no. 17:7255-7262. PNNL-SA-123271. doi:10.1021/acs.chemmater.7b01847
Wan C., S. Xu, M.Y. Hu, R. Cao, J. Qian, Z. Qin, and J. Liu, et al. 2017. "Multinuclear NMR Study of the Solid Electrolyte Interface Formed in Lithium Metal Batteries." ACS Applied Materials & Interfaces 9, no. 17:14741-14748. PNNL-SA-122289. doi:10.1021/acsami.6b15383
Xiao X., M.Y. Hu, X. Zhang, and J.Z. Hu. 2017. "NMR-based Metabolomics Analysis of Liver from C57BL/6 Mouse Exposed to Ionizing Radiation." Radiation Research 188, no. 1:44-55. PNNL-SA-120056. doi:10.1667/RR14602.1
Zhao Z., H. Shi, C. Wan, M.Y. Hu, Y. Liu, D. Mei, and D.M. Camaioni, et al. 2017. "“Mechanism of Phenol Alkylation in Zeolite H-BEA Using In Situ Solid-State NMR Spectroscopy”." Journal of the American Chemical Society 139, no. 27:9178-9185. PNNL-SA-122818. doi:10.1021/jacs.7b02153

2016

Baker C., J.L. Gole, J.I. Brauer, S. Graham, J.Z. Hu, J. Kenvin, and A.D. D'Amico, et al. 2016. "Activity of titania and zeolite samples dosed with triethylamine." Microporous and Mesoporous Materials 220. PNNL-SA-105966. doi:10.1016/j.micromeso.2015.08.022
Deng X., M.Y. Hu, X. Wei, W. Wang, K.T. Mueller, Z. Chen, and J.Z. Hu. 2016. "Nuclear Magnetic Resonance Studies of the Solvation Structures of a High-Performance Nonaqueous Redox Flow Electrolyte." Journal of Power Sources 308. PNNL-SA-113232. doi:10.1016/j.jpowsour.2015.12.005
Han K., N. Rajput, M. Vijayakumar, X. Wei, W. Wang, J.Z. Hu, and K.A. Persson, et al. 2016. "Preferential Solvation of an Asymmetric Redox Molecule." Journal of Physical Chemistry C 120, no. 49:27834-27839. PNNL-SA-113547. doi:10.1021/acs.jpcc.6b09114
Hu J.Z. 2016. "Magic Angle Spinning NMR Metabolomics." Metabolomics 6, no. 2:e147. PNNL-SA-118614. doi:10.4172/2153-0769.1000e147
Hu J.Z., S. Xu, J. Kwak, M.Y. Hu, C. Wan, Z. Zhao, and J. Szanyi, et al. 2016. "High Field 27Al MAS NMR and TPD studies of active sites in ethanol dehydration using thermally treated transitional aluminas as catalysts." Journal of Catalysis 336, no. 1:85-93. PNNL-SA-106119. doi:10.1016/j.jcat.2016.01.006
Hu J.Z., S. Xu, J. Kwak, M.Y. Hu, C. Wan, Z. Zhao, and J. Szanyi, et al. 2016. "High field 27Al MAS NMR and TPD studies of active sites in ethanol dehydration using thermally treated transitional aluminas as catalysts." Journal of Catalysis 336. PNNL-SA-110979. doi:10.1016/j.jcat.2016.01.006
Hu J.Z., X. Xiao, and M.Y. Hu. 2016. "NMR Metabolomics in Ionizing Radiation." Clinics in Oncology 1. PNNL-SA-120277.
Hu J.Z., Z. Zhao, M.Y. Hu, J. Feng, X. Deng, X. Chen, and W. Xu, et al. 2016. "In situ 7Li and 133Cs Nuclear Magnetic Resonance Investigations on the Role of Cs+ Additive in Lithium-Metal Deposition Process." Journal of Power Sources 304. PNNL-SA-110396. doi:10.1016/j.jpowsour.2015.10.067
Hu M.Y., X. Deng, S. Thanthiriwatte, V.E. Jackson, C. Wan, O. Qafoku, and D.A. Dixon, et al. 2016. "In Situ Natural Abundance 17O and 25Mg NMR Investigation of Aqueous Mg(OH)2 Dissolution in the Presence of Supercritical CO2." Environmental Science & Technology 50, no. 22:12373-12384. PNNL-SA-118648. doi:10.1021/acs.est.6b03443
Qian J., B.D. Adams, J. Zheng, W. Xu, W.A. Henderson, J. Wang, and M.E. Bowden, et al. 2016. "Anode-Free Rechargeable Lithium Metal Batteries." Advanced Functional Materials 26, no. 39:7094-7102. PNNL-SA-117788. doi:10.1002/adfm.201602353
Tang W., B. Goh, M.Y. Hu, C. Wan, B. Tian, X. Deng, and C. Peng, et al. 2016. "In Situ Raman and Nuclear Magnetic Resonance Study of Trapped Lithium in the Solid Electrolyte Interface of Reduced Graphene Oxide." Journal of Physical Chemistry C 120, no. 5:2600-2608. PNNL-ACT-SA-10132. doi:10.1021/acs.jpcc.5b12551
Wan C., M.Y. Hu, N.R. Jaegers, D. Shi, H. Wang, F. Gao, and Z. Qin, et al. 2016. "Investigating the Surface Structure of ?-Al2O3 Supported WOx Catalysts by High-Field 27Al MAS NMR and Electronic Structure Calculations." Journal of Physical Chemistry C 120, no. 40:23093-23103. PNNL-SA-119580. doi:10.1021/acs.jpcc.6b09060
Wan C., M.Y. Hu, O. Borodin, J. Qian, Z. Qin, J. Zhang, and J.Z. Hu. 2016. "Natural Abundance 17O, 6Li NMR and Molecular Modeling Studies of the Solvation Structures of Lithium bis(fluorosulfonyl)imide/1,2-dimethoxyethane Liquid Electrolytes." Journal of Power Sources 307. PNNL-SA-113087. doi:10.1016/j.jpowsour.2015.12.120
Xiao X., M.Y. Hu, M. Liu, and J.Z. Hu. 2016. "1H NMR Metabolomics Study of Spleen from C57BL/6 Mice Exposed to Gamma Radiation." Metabolomics 6, no. 1:Article No. 165. PNNL-SA-119978. doi:10.4172/2153-0769.1000165
Xu S., Z. Zhao, M.Y. Hu, X. Han, J.Z. Hu, and X. Bao. 2016. "Investigation Of Water Assisted Phase Transformation Process From AlPO4-5 to AlPO4-tridymite." Microporous and Mesoporous Materials 223. PNNL-SA-115503. doi:10.1016/j.micromeso.2015.10.039
Zhao Z., S. Xu, M.Y. Hu, X. Bao, and J.Z. Hu. 2016. "In situ High Temperature High Pressure MAS NMR Study on the Crystallization of AlPO4-5." Journal of Physical Chemistry C 120, no. 3:1701-1708. PNNL-SA-110249. doi:10.1021/acs.jpcc.5b11294

2015

Deng X., M.Y. Hu, X. Wei, W. Wang, Z. Chen, J. Liu, and J.Z. Hu. 2015. "Natural Abundance 17O Nuclear Magnetic Resonance and Computational Modeling Studies of Lithium Based Liquid Electrolytes." Journal of Power Sources 285. PNNL-SA-105759. doi:10.1016/j.jpowsour.2015.03.091
Hu J.Z., M.Y. Hu, Z. Zhao, S. Xu, A. Vjunov, H. Shi, and D.M. Camaioni, et al. 2015. "Sealed Rotors for In Situ High Temperature High Pressure MAS NMR." Chemical Communications 51, no. 70:13458-13461. PNNL-SA-110035. doi:10.1039/c5cc03910j
Hu J.Z., S. Xu, W. Li, M.Y. Hu, X. Deng, D.A. Dixon, and M. Vasiliu, et al. 2015. "Investigation of the Structure and Active Sites of TiO2 Nanorod Supported VOx Catalysts by High-Field and Fast-Spinning 51V MASNMR." ACS Catalysis 5, no. 7:3945-3952. PNNL-SA-107998. doi:10.1021/acscatal.5b00286
Hu J.Z., X. Wang, J. Feng, B.M. Webb-Robertson, K.M. Waters, S.C. Tilton, and J.G. Pounds, et al. 2015. "Metabolite Signatures in Hydrophilic Extracts of Mouse Lungs Exposed to Cigarette Smoke Revealed By 1H NMR Metabolomics Investigation." Metabolomics 5, no. 2:Article No. 143. PNNL-SA-102290. doi:10.4172/2153-0769.1000143
Kovarik L., M.E. Bowden, D. Shi, N.M. Washton, A. Anderson, J.Z. Hu, and J. Lee, et al. 2015. "Unraveling the Origin of Structural Disorder in High Temperature Transition Al2O3: Structure of ?-Al2O3." Chemistry of Materials 27, no. 20:7042-7049. PNNL-SA-111174. doi:10.1021/acs.chemmater.5b02523
Liu T.L., J.T. Cox, D. Hu, X. Deng, J.Z. Hu, M.Y. Hu, and J. Xiao, et al. 2015. "A Fundamental Study on the [(µ-Cl)3Mg2(THF)6]+ Dimer Electrolytes for Rechargeable Mg Batteries." Chemical Communications 51, no. 12:2312-2315. PNNL-SA-104532. doi:10.1039/c4cc07621d
Tang W., Y. Liu, C. Peng, M.Y. Hu, X. Deng, M. Lin, and J.Z. Hu, et al. 2015. "Probing Lithium Germanide Phase Evolution and Structural Change in a Germanium-in-Carbon Nanotube Energy Storage System." Journal of the American Chemical Society 137, no. 7:2600-7. PNNL-ACT-SA-10046. doi:10.1021/ja5116259
Vijayakumar M., Z. Nie, E.D. Walter, J.Z. Hu, J. Liu, V.L. Sprenkle, and W. Wang. 2015. "Understanding Aqueous Electrolyte Stability through Combined Computational and Magnetic Resonance Spectroscopy: A Case Study on Vanadium Redox Flow Battery Electrolytes." ChemPlusChem 80, no. 2:428-437. PNNL-SA-102555. doi:10.1002/cplu.201402139
Vjunov A., J.L. Fulton, D.M. Camaioni, J.Z. Hu, S.D. Burton, I. Arslan, and J.A. Lercher. 2015. "Impact of aqueous medium on zeolite framework integrity." Chemistry of Materials 27, no. 9:3533-3545. PNNL-SA-107354. doi:10.1021/acs.chemmater.5b01238
Vjunov A., J.L. Fulton, T. Huthwelker, S. Pin, D. Mei, G.K. Schenter, and N. Govind, et al. 2015. "Correction to “Quantitatively probing the Al distribution in zeolites”." Journal of the American Chemical Society 137, no. 6:2409. PNNL-SA-107353. doi:10.1021/ja513077w
Wei X., L. Cosimbescu, W. Xu, J.Z. Hu, M. Vijayakumar, J. Feng, and M.Y. Hu, et al. 2015. "Towards High-Performance Nonaqueous Redox Flow Electrolyte through Ionic Modification of Active Species." Advanced Energy Materials 5, no. 1:Article No. 1400678. PNNL-SA-97506. doi:10.1002/aenm.201400678
Xiao J., J.Z. Hu, H. Chen, M. Vijayakumar, J. Zheng, H. Pan, and E.D. Walter, et al. 2015. "Following the Transient Reactions in Lithium-Sulfur Batteries Using In an In Situ Nuclear Magnetic Resonance Technique." Nano Letters 15, no. 5:3309-3316. PNNL-SA-101779. doi:10.1021/acs.nanolett.5b00521
Xu S., E.D. Walter, Z. Zhao, M.Y. Hu, X. Han, J.Z. Hu, and X. Bao. 2015. "Dynamic Structural Changes of SiO2 Supported Pt-Ni Bimetallic Catalysts over Redox Treatments Revealed by NMR and EPR." Journal of Physical Chemistry C 119, no. 36:21219-21226. PNNL-SA-112670. doi:10.1021/acs.jpcc.5b06344
Zhao Z., S. Xu, M.Y. Hu, X. Bao, C.H. Peden, and J.Z. Hu. 2015. "Investigation of Aluminum Site Changes of Dehydrated Zeolite H-Beta during a Rehydration Process by High Field Solid State NMR." Journal of Physical Chemistry C 119, no. 3:1410-1417. PNNL-SA-105728. doi:10.1021/jp509982r

2014

Chen X., X. Li, D. Mei, J. Feng, M.Y. Hu, J.Z. Hu, and M.H. Engelhard, et al. 2014. "Reduction Mechanism of Fluoroethylene Carbonate for Stable Solid-Electrolyte Interphase Film on Silicon Anode." ChemSusChem 7, no. 2:549-554. PNNL-SA-97198. doi:10.1002/cssc.201300770
Han K., N. Rajput, X. Wei, W. Wang, J.Z. Hu, K.A. Persson, and K.T. Mueller. 2014. "Diffusional Motion of Redox Centers in Carbonate Electrolytes." Journal of Chemical Physics 141, no. 10:104509. PNNL-SA-103453. doi:10.1063/1.4894481
Lercher J.A., A.M. Appel, T. Autrey, R.M. Bullock, D.M. Camaioni, H.M. Cho, and D.A. Dixon, et al. 2014. "Multifunctional Catalysts to Synthesize and Utilize Energy Carriers." In Frontiers at the Interface between Homogeneous and Heterogeneous Catalysis, II, 207-219. Washington, District Of Columbia:U.S. Department of Energy, Office of Science. PNNL-SA-103068.
Liu T.L., Y. Shao, G. Li, M. Gu, J.Z. Hu, S. Xu, and Z. Nie, et al. 2014. "A Facile Approach Using MgCl2 to Formulate High Performance Mg2+ Electrolytes for Rechargeable Mg Batteries." Journal of Materials Chemistry A 2, no. 10:3430 - 3438. PNNL-SA-98069. doi:10.1039/c3ta14825d
Qafoku O., J.Z. Hu, N.J. Hess, M.Y. Hu, E.S. Ilton, J. Feng, and B.W. Arey, et al. 2014. "Formation of Submicron Magnesite during Reaction of Natural Forsterite in H2O-Saturated Supercritical CO2." Geochimica et Cosmochimica Acta 134. PNNL-SA-93839. doi:10.1016/j.gca.2013.09.024
Qu Y., J. Feng, S. Deng, L. Cao, Q. Zhang, R. Zhao, and Z. Zhang, et al. 2014. "Structural Analysis of N- and O-glycans Using ZIC-HILIC/Dialysis Coupled to NMR Detection." Fungal Genetics and Biology : FG & B 72. PNNL-SA-101957. doi:10.1016/j.fgb.2014.08.001
Shao Y., N. Rajput, J.Z. Hu, M.Y. Hu, T.L. Liu, Z. Wei, and M. Gu, et al. 2014. "Nanocomposite polymer electrolyte for rechargeable magnesium batteries." Nano Energy 2015, no. 12:750-759. PNNL-SA-103424. doi:10.1016/j.nanoen.2014.12.028
Vijayakumar M., B. Schwenzer, V. Shutthanandan, J.Z. Hu, J. Liu, and I.A. Aksay. 2014. "Elucidating graphene - Ionic Liquid interfacial region: a combined experimental and computational study." Nano Energy 3. PNNL-SA-87010. doi:10.1016/j.nanoen.2012.09.014
Vjunov A., J.L. Fulton, T. Huthwelker, S. Pin, D. Mei, G.K. Schenter, and N. Govind, et al. 2014. "Quantitatively Probing the Al Distribution in Zeolites." Journal of the American Chemical Society 136, no. 23:8296-8306. PNNL-SA-100687. doi:10.1021/ja501361v
Vjunov A., M.Y. Hu, J. Feng, D.M. Camaioni, D. Mei, J.Z. Hu, and C. Zhao, et al. 2014. "Following Solid-Acid-Catalyzed Reactions by MAS NMR Spectroscopy in Liquid Phase -Zeolite-Catalyzed Conversion of Cyclohexanol in Water." Angewandte Chemie International Edition 53, no. 2:479-482. PNNL-SA-96916. doi:10.1002/anie.201306673
Wang X., M.Y. Hu, J. Feng, M. Liu, and J.Z. Hu. 2014. "1H NMR Metabolomics Study of Metastatic Melanoma in C57BL/6J Mouse Spleen." Metabolomics 10, no. 6:1129-1144. PNNL-SA-101943. doi:10.1007/s11306-014-0652-z
Wang X., M.Y. Hu, M. Liu, and J.Z. Hu. 2014. "Metastatic Melanoma Induced Metabolic Changes in C57BL/6J Mouse Stomach Measured by 1H NMR Spectroscopy." Metabolomics 4, no. 2:135. PNNL-SA-105912. doi:10.4172/2153-0769.1000135
Xiao J., P. Meduri, H. Chen, Z. Wang, F. Gao, J.Z. Hu, and J. Feng, et al. 2014. "Energetics of Defects on Graphene through Fluorination." ChemSusChem 7, no. 5:1295-1300. PNNL-SA-92043. doi:10.1002/cssc.201301066

2013

Feng J., J.Z. Hu, S.D. Burton, and D.W. Hoyt. 2013. "High Resolution Magic Angle Spinning 1H-NMR Metabolic Profiling of Nanoliter Biological Tissues at High Magnetic Field." Chinese Journal of Magnetic Resonance 30, no. 1:1-11. PNNL-SA-89007.
Feng J., N.G. Isern, S.D. Burton, and J.Z. Hu. 2013. "Studies of Secondary Melanoma on C57BL/6J Mouse Liver Using 1H NMR Metabolomics." Metabolites 3. PNNL-SA-93339. doi:10.3390/metabo3041011
Liu J., J. Zhang, Z. Yang, J.P. Lemmon, C.H. Imhoff, G.L. Graff, and L. Li, et al. 2013. "Materials Science and Materials Chemistry for Large Scale Electrochemical Energy Storage: From Transportation to Electrical Grid." Advanced Functional Materials 23, no. 8:929-946. PNNL-SA-87308. doi:10.1002/adfm.201200690
Loring J.S., H.T. Schaef, C.J. Thompson, R.V. Turcu, Q.R. Miller, J. Chen, and J.Z. Hu, et al. 2013. "Clay hydration/dehydration in dry to water-saturated supercritical CO2: Implications for caprock integrity." Energy Procedia 37. PNNL-SA-91508. doi:10.1016/j.egypro.2013.06.463
Miller Q., C.J. Thompson, J.S. Loring, C.F. Windisch, M.E. Bowden, D.W. Hoyt, and J.Z. Hu, et al. 2013. "Insights into Silicate Carbonation Processes in Water-Bearing Supercritical CO2 Fluids." International Journal of Greenhouse Gas Control 15. PNNL-SA-89916. doi:10.1016/j.ijggc.2013.02.005
Turcu R.V., D.W. Hoyt, K.M. Rosso, J.A. Sears, J.S. Loring, A.R. Felmy, and J.Z. Hu. 2013. "Rotor Design for High Pressure Magic Angle Spinning Nuclear Magnetic Resonance." Journal of Magnetic Resonance 226. PNNL-SA-88703. doi:10.1016/j.jmr.2012.08.009
Vijayakumar M., and J.Z. Hu. 2013. "Exploring the interaction between lithium ion and defective graphene surface using dispersion corrected DFT studies." ECS Transactions 53, no. 10:23-32. PNNL-SA-91592. doi:10.1149/05310.0023ecst
Vijayakumar M., W. Wang, Z. Nie, V.L. Sprenkle, and J.Z. Hu. 2013. "Elucidating the Higher Stability of Vanadium (V) Cations in Mixed Acid Based Redox Flow Battery Electrolytes." Journal of Power Sources 241. PNNL-SA-95082. doi:10.1016/j.jpowsour.2013.04.072

2012

Felmy A.R., O. Qafoku, B.W. Arey, J.Z. Hu, M.Y. Hu, H.T. Schaef, and E.S. Ilton, et al. 2012. "Reaction of Water-Saturated Supercritical CO2 with Forsterite: Evidence for Magnesite Formation at Low Temperatures." Geochimica et Cosmochimica Acta 91. PNNL-SA-82433. doi:10.1016/j.gca.2012.05.026
Hu J.Z., J.A. Sears, H.S. Mehta, J.J. Ford, J. Kwak, K. Zhu, and Y. Wang, et al. 2012. "A Large Sample Volume Magic Angle Spinning Nuclear Magnetic Resonance Probe for In-Situ Investigations with Constant Flow of Reactants." Physical Chemistry Chemical Physics. PCCP 14, no. 7:2137-2143. PNNL-SA-82533. doi:10.1039/c1cp22692d
Hu M.Y., J. Feng, D.M. Camaioni, R.V. Turcu, C.H. Peden, J.A. Lercher, and J.Z. Hu. 2012. "IN-SITU MAGIC ANGLE SPINNING NMR INVESTIGATIONS ON CATALYTIC CONVERSION OF BIOGENIC MOLECULES IN THE PRESENCE OF AQUEOUS WATER." In Proceedings of the 244th American Chemical Society National Meeting and Exposition, Division of Petroleum Chemistry, August 19-23, 2012, Philadelphia, PA, 57, 215-217. Washington Dc:American Chemical Society. PNNL-SA-92029.
Kottman R.M., A.A. Kulkarni, K.A. Smolnycki, E. Lyda, T. Dahanayake, R. Salibi, and S. Honnons, et al. 2012. "Lactic Acid is Elevated in Idiopathic Pulmonary Fibrosis and Induces Myofibroblast Differentiation Via pH-Dependent Activation of Transforming Growth Factor-ß." American Journal of Respiratory and Critical Care Medicine 186, no. 8:740-751. PNNL-SA-89313. doi:10.1164/rccm.201201-0084OC
Loring J.S., H.T. Schaef, R.V. Turcu, C.J. Thompson, Q. Miller, P.F. Martin, and J.Z. Hu, et al. 2012. "In Situ Molecular Spectroscopic Evidence for CO2 Intercalation into Montmorillonite in Supercritical Carbon Dioxide." Langmuir 28, no. 18:7125-7128. PNNL-SA-86500. doi:10.1021/la301136w
She X., J. Kwak, J. Sun, J.Z. Hu, M.Y. Hu, C.M. Wang, and C.H. Peden, et al. 2012. "Highly Dispersed and Active ReOx on Alumina-Modified SBA-15 Silica for 2-Butanol Dehydration." ACS Catalysis 2, no. 6:1020-1026. PNNL-SA-84678. doi:10.1021/cs2006444
Vijayakumar M., B. Schwenzer, S. Kim, Z. Yang, S. Thevuthasan, J. Liu, and G.L. Graff, et al. 2012. "Investigation of Local Environments in Nafion-SiO2 Composite Membranes used in Vanadium Redox Flow Batteries." Solid State Nuclear Magnetic Resonance 42. PNNL-SA-80357. doi:10.1016/j.ssnmr.2011.11.005
Vijayakumar M., L. Li, Z. Nie, Z. Yang, and J.Z. Hu. 2012. "Structure and Stability of Hexa-Aqua V(III) Cations in Vanadium Redox Flow Battery Electrolytes." Physical Chemistry Chemical Physics. PCCP 14, no. 29:10233-10242. PNNL-SA-86137. doi:10.1039/c2cp40707h
Xu W., J.Z. Hu, M.H. Engelhard, S.A. Towne, J.S. Hardy, J. Xiao, and J. Feng, et al. 2012. "The Stability of Organic Solvents and Carbon Electrode in Nonaqueous Li-O2 Batteries." Journal of Power Sources 215. PNNL-SA-85748. doi:10.1016/j.jpowsour.2012.05.021

2011

Hoyt D.W., R.V. Turcu, J.A. Sears, K.M. Rosso, S.D. Burton, A.R. Felmy, and J.Z. Hu. 2011. "High-pressure Magic Angle Spinning Nuclear Magnetic Resonance." Journal of Magnetic Resonance 212, no. 2:378-385. PNNL-SA-80681. doi:10.1016/j.jmr.2011.07.019
Hoyt D.W., R.V. Turcu, J.A. Sears, K.M. Rosso, S.D. Burton, J. Kwak, and A.R. Felmy, et al. 2011. "IN SITU MAGIC ANGLE SPINNING NMR FOR STUDYING GEOLOGICAL CO(2) SEQUESTRATION." In 241st National Meeting and Exposition of the American Chemical Society, March 27-31, 2011, Anaheim, California, 241, 245-Fuel. Washington Dc:American Chemical Society. PNNL-SA-77039.
Hu J.Z. 2011. "Slow Magic Angle Sample Spinning: A Non- or Minimally Invasive Method for High- Resolution 1H Nuclear Magnetic Resonance (NMR) Metabolic Profiling." In Metabolic Profiling: Methods and Protocols. Methods in Molecular Biology, edited by TO Metz. 335-364. New York, New York:Humana Press. PNNL-SA-70771.
Hu J.Z., J. Kwak, Y. Wang, M.Y. Hu, R.V. Turcu, and C.H. Peden. 2011. "Characterizing Surface Acidic Sites in Mesoporous-Silica-Supported Tungsten Oxide Catalysts Using Solid State NMR and Quantum Chemistry Calculations." Journal of Physical Chemistry C 115, no. 47:23354-23362. PNNL-SA-71974. doi:10.1021/jp203813f
Kwak J., J.Z. Hu, R.V. Turcu, K.M. Rosso, E.S. Ilton, C.M. Wang, and J.A. Sears, et al. 2011. "The Role of H2O in the Carbonation of Forsterite in Supercritical CO2." International Journal of Greenhouse Gas Control 5, no. 4:1081-1092. PNNL-SA-76665. doi:10.1016/j.ijggc.2011.05.013
Li L., S. Kim, W. Wang, M. Vijayakumar, Z. Nie, B. Chen, and J. Zhang, et al. 2011. "A Stable Vanadium Redox-Flow Battery with High Energy Density for Large-scale Energy Storage." Advanced Energy Materials 1, no. 3:394-400. PNNL-SA-75871.
Vijayakumar M., B.M. Sivakumar, P. Nachimuthu, B. Schwenzer, S. Kim, Z. Yang, and J. Liu, et al. 2011. "Spectroscopic Investigations of the Fouling Process on Nafion Membranes in Vanadium Redox Flow Batteries." Journal of Membrane Science 366, no. 1-2:325-334. PNNL-SA-73754. doi:10.1016/j.memsci.2010.10.018
Vijayakumar M., L. Li, G.L. Graff, J. Liu, H. Zhang, Z. Yang, and J.Z. Hu. 2011. "Towards Understanding the Poor Thermal Stability of V5+ Electrolyte Solution in Vanadium Redox Flow Batteries." Journal of Power Sources 196, no. 7:3669-3672. PNNL-SA-75255. doi:10.1016/j.jpowsour.2010.11.126
Vijayakumar M., S.N. Kerisit, K.M. Rosso, S.D. Burton, J.A. Sears, Z. Yang, and G.L. Graff, et al. 2011. "Lithium Diffusion in Li4Ti5O12 at High Temperatures." Journal of Power Sources 196, no. 4:2211-2220. PNNL-SA-70935.
White M.D., B.P. McGrail, H.T. Schaef, J.Z. Hu, D.W. Hoyt, A.R. Felmy, and K.M. Rosso, et al. 2011. "Multiphase Sequestration Geochemistry: Model for Mineral Carbonation." Energy Procedia 4. PNNL-SA-74658. doi:10.1016/j.egypro.2011.02.472
Xiao J., J.Z. Hu, D. Wang, D. Hu, W. Xu, G.L. Graff, and Z. Nie, et al. 2011. "Investigation of the Rechargeability of Li-O2 Batteries in Non-aqueous Electrolyte." Journal of Power Sources 196, no. 13:5674-5678. PNNL-SA-75791.
Zhu K., J. Sun, J. Liu, L.Q. Wang, H. Wan, J.Z. Hu, and Y. Wang, et al. 2011. "Solvent Evaporation Assisted Preparation of Oriented Nanocrystalline Mesoporous MFI Zeolites." ACS Catalysis 1, no. 7:682-690. PNNL-SA-75369. doi:10.1021/cs200085e

2010

Hu J.Z., J. Kwak, Z. Yang, X. Wan, and L.D. Shaw. 2010. "Detailed Investigation of Ion Exchange in Ball Milled LiH+MgB2 System using Ultra-High Field NMR Spectroscopy." Journal of Power Sources 195, no. 11:3645-3648. PNNL-SA-70035. doi:10.1016/j.jpowsour.2009.12.033
Kwak J., J.Z. Hu, D.W. Hoyt, J.A. Sears, C.M. Wang, K.M. Rosso, and A.R. Felmy. 2010. "Metal Carbonation of Forsterite in Supercritical CO2 and H2O Using Solid State 29Si, 13C NMR Spectroscop." Journal of Physical Chemistry C 114, no. 9:4126 - 4134. PNNL-SA-68897. doi:10.1021/jp1001308
Mei D., J. Kwak, J.Z. Hu, S. Cho, J. Szanyi, L. Allard, and C.H. Peden. 2010. "The Unique Role of Anchoring Penta-coordinated Al3+ Sites in the Sintering of ? Al2O3-supported Pt Catalysts." The Journal of Physical Chemistry Letters 1. PNNL-SA-71486. doi:10.1021/jz101073p
Shaw L.L., X. Wan, J.Z. Hu, J. Kwak, and Z. Yang. 2010. "Solid-State Hydriding Mechanism in the LiBH4 + MgH2 System." Journal of Physical Chemistry C 114, no. 17:8089-8098. PNNL-SA-71617. doi:10.1021/jp1003837
Vijayakumar M., S.D. Burton, C. Huang, L. Li, Z. Yang, G.L. Graff, and J. Liu, et al. 2010. "Nuclear Magnetic Resonance Studies on Vanadium(IV) Electrolyte Solutions for Vanadium Redox Flow Battery." Journal of Power Sources 195, no. 22 SP ISS:7709-7717. PNNL-SA-71574.

2009

Baer D.R., M.H. Engelhard, A.R. Felmy, J.J. Ford, J.Z. Hu, A.S. Lea, and P. Nachimuthu, et al. 2009. "New Approaches for Characterizing Sensor and Other Modern Complex Materials." ECS Transactions 19, no. 6:137-148. PNNL-SA-65017. doi:10.1149/1.3118546
Hu J.Z., J. Kwak, Y. Wang, C.H. Peden, H. Zheng, D. Ma, and X. Bao. 2009. "Studies of the Active Sites for Methane Dehydroaromatization Using Ultrahigh-Field Solid-State Mo95 NMR Spectroscopy." Journal of Physical Chemistry C 113, no. 7:2936-2942. PNNL-SA-62099. doi:10.1021/jp8107914
Hu J.Z., J. Kwak, Z. Yang, X. Wan, and L.D. Shaw. 2009. "Direct Observation of Ion Exchange in Mechanically Activated LiH+MgB2 System Using Ultra-High Field Nuclear Magnetic Resonance Spectroscopy." Applied Physics Letters 94, no. 14:Art No.: 141905. PNNL-SA-62265. doi:10.1063/1.3110966
Hu J.Z., J.A. Sears, J. Kwak, D.W. Hoyt, Y. Wang, and C.H. Peden. 2009. "An Isotropic Chemical Shift-Chemical Shift Anisotropic Correlation Experiment Using Discrete Magic Angle Turning." Journal of Magnetic Resonance 198, no. 1:105-110. PNNL-SA-63634.
Kwak J., J.Z. Hu, D. Mei, C.W. Yi, D. Kim, C.H. Peden, and L. Allard, et al. 2009. "Coordinatively unsaturated Al3+ centers as binding sites for active catalyst phases on ?-Al2O3." Science 325, no. 5948:1670-1673. PNNL-SA-67165. doi:10.1126/science.1176745
Osborn W., T. Markmaitree, L.D. Shaw, J.Z. Hu, J. Kwak, and Z. Yang. 2009. "Low Temperature Milling of the LiNH2 + LiH Hydrogen Storage System." International Journal of Hydrogen Energy 34, no. 10:4331-4339. PNNL-SA-65424. doi:10.1016/j.ijhydene.2009.03.032
Osborn W., T. Markmaitree, L.D. Shaw, R. Ren, J.Z. Hu, J. Kwak, and Z. Yang. 2009. "Solid-State Hydrogen Storage: Storage Capacity,Thermodynamics and Kinetics." JOM. The Journal of the Minerals, Metals and Materials Society 61, no. 4:45-51. PNNL-SA-65236.
Vijayakumar M., S.N. Kerisit, C.M. Wang, Z. Nie, K.M. Rosso, Z. Yang, and G.L. Graff, et al. 2009. "Effect of Chemical Lithium Intercalation into Rutile TiO2 Nanorods." Journal of Physical Chemistry C 113, no. 32:14567-14574. PNNL-SA-66004. doi:10.1021/jp904148z
Vijayakumar M., S.N. Kerisit, Z. Yang, G.L. Graff, J. Liu, J.A. Sears, and S.D. Burton, et al. 2009. "A Combined 6,7Li NMR and Molecular Dynamics Study of Li Diffusion in Li2TiO3." Journal of Physical Chemistry C 113, no. 46:20108-20116. PNNL-SA-67583. doi:10.1021/jp9072125
Webb-Robertson B.M., L.A. McCue, N. Beagley, J.E. McDermott, D.S. Wunschel, S.M. Varnum, and J.Z. Hu, et al. 2009. "A Bayesian Integration Model of High-Throughput Proteomics and Metabolomics Data for Improved Early Detection of Microbial Infections." In Pacific Symposium on Biocomputing, 14, 451-463. Singapore:World Scientific Publishing Co. PNNL-SA-61531.
Zhang Q., J.Z. Hu, D.N. Rommereim, M.K. Murphy, R.P. Phipps, D.L. Huso, and J.F. Dicello. 2009. "Application of High-Resolution H-1 MAS NMR Spectroscopy to the Analysis of Intact Bones from Mice Exposed to Gamma Radiation." Radiation Research 172, no. 5:607-616. PNWD-SA-8286. doi:10.1667/RR1715.1
Zhu K., J.Z. Hu, X. She, J. Liu, Z. Nie, Y. Wang, and C.H. Peden, et al. 2009. "Characterization of Dispersed Heteropoly Acid on Mesoporous Zeolite Using Solid-State P-31 NMR Spin-Lattice Relaxation." Journal of the American Chemical Society 131, no. 28:9715-9721. PNNL-SA-68413. doi:10.1021/ja901317r

2008

Herrera J.E., J. Kwak, J. Hu, Y. Wang, and C.H. Peden. 2008. "Effects of novel supports on the physical and catalytic properties of tungstophosphoric acid for alcohol dehydration reactions." Topics in Catalysis 49, no. 3-4:259-267. PNNL-SA-57700. doi:10.1007/s11244-008-9081-4
Hu J., D.N. Rommereim, K.R. Minard, A. Woodstock, B.J. Harrer, R.A. Wind, and R.P. Phipps, et al. 2008. "Metabolomics in Lung Inflammation: A High Resolution ¹H NMR Study of Mice Exposed to Silica Dust." Toxicology Mechanisms and Methods 18, no. 5:385-398. PNWD-SA-7807. doi:10.1080/15376510701611032
Hu J., J. Kwak, Z. Yang, W. Osborn, T. Markmaitree, and L.D. Shaw. 2008. "Investigation of Mechanical Activation on Li-N-H Systems Using 6Li Magic Angle Spinning Nuclear Magnetic Resonance at Ultra-High Field." Journal of Power Sources 182, no. 1:278-283. PNNL-SA-58038.
Hu J., J. Kwak, Z. Yang, w. osborn, T. Markmaitree, and L.D. Shaw. 2008. "Probing the Reaction Pathway of Dehydrogenation of the LiNH2 + LiH Mixture Using In Situ 1H NMR Spectroscopy." Journal of Power Sources 181, no. 1:116-119. PNNL-SA-59762.
Kwak J., J. Hu, A.C. Lukaski, D. Kim, J. Szanyi, and C.H. Peden. 2008. "The Role of PentaCoordinated Al3+ Ions in the High Temperature Phase Transformation of ?-Al2O3." Journal of Physical Chemistry C 112, no. 25:9486-9492. PNNL-SA-58543. doi:10.1021/jp802631u
Zheng H., D. Ma, X. Bao, J. Hu, J. Kwak, Y. Wang, and C.H. Peden. 2008. "Direct Observation of the Active Center for Methane Dehydroaromatization Using an Ultrahigh Field 95Mo NMR Spectroscopy." Journal of the American Chemical Society 130, no. 12:3722-3723. PNNL-SA-57408. doi:10.1021/ja7110916

2007

Dixon D.A., Z. Dohnalek, M.S. Gutowski, J. Hu, E. Iglesia, B.D. Kay, and J. Liu, et al. 2007. "Early Transition Metal Oxides as Catalysts: Crossing Scales from Clusters to Single Crystals to Functioning Materials." In Frontiers in Catalysis Science. Meeting of the Catalysis and Chemical Transformations Program Chemical Sciences, Geosciences and Biosciences Division, Office of Basic Energy Sciences, U.S. Department of Energy Rockville, MD May 23-26, 2004, 389-392. Washington, District Of Columbia:Department of Energy. PNNL-SA-54459.
Kwak J., J. Hu, D. Kim, J. Szanyi, and C.H. Peden. 2007. "Penta-coordinated Al3+ ions as preferential nucleation sites for BaO on ?-Al2O3: an ultra-high magnetic field 27Al MAS NMR study." Journal of Catalysis 251, no. 2:189-194. PNNL-SA-54213. doi:10.1016/j.jcat.2007.06.029
Lu C., J. Hu, J. Kwak, Z. Yang, R. Ren, T. Markmaitree, and L.D. Shaw. 2007. "Study the Effects of Mechanical Activation on Li-N-H Systems With 1H and 6Li Solid-State NMR." Journal of Power Sources 170, no. 2:419-424. PNNL-SA-53592. doi:10.1016/j.jpowsour.2007.02.080

2006

Herrera J.E., J. Kwak, J. Hu, Y. Wang, and C.H. Peden. 2006. "Synthesis of Nanodispersed Oxides of Vanadium, Titanium, Molybdenum, and Tungsten on Mesoporous Silica using Atomic Layer Deposition." Topics in Catalysis 39, no. 3-4:245-255. PNNL-SA-46144. doi:10.1007/s11244-006-0063-0
Herrera J.E., J. Kwak, J. Hu, Y. Wang, C.H. Peden, J. Macht, and E. Iglesia. 2006. "Synthesis, Characterization, and Catalytic Function of Novel Highly Dispersed Tungsten Oxide Catalysts on Mesoporous Silica." Journal of Catalysis 239, no. 1:200-211. PNNL-SA-46575.
Hu J., D.N. Rommereim, R.A. Wind, K.R. Minard, and J.A. Sears. 2006. "A Simple Approach for Obtaining High Resolution, High Sensitivity ¹H NMR Metabolite Spectra of Biofluids with Limited Mass Supply." In Proceedings of the 2006 International Conference on Bioinformatics and Computational Biology (BIOCOMP '06), edited by HR Arabnia and H. Valafar, 360-366. Las Vegas, Nevada:CSREA Press. PNNL-SA-48823. A Simple Approach for Obtaining High Resolution, High Sensitivity ¹H NMR Metabolite Spectra of Biofluids with Limited Mass Supply
Hu J., R.A. Wind, and D.N. Rommereim. 2006. "H-1 Relaxation Times of Metabolites in Biological Samples Obtained with Nondestructive Ex-vivo Slow-MAS NMR." Magnetic Resonance in Chemistry 44, no. 3:269-275. PNNL-SA-46426. doi:10.1002/mrc.1764
Kwak J., J.E. Herrera, J. Hu, Y. Wang, and C.H. Peden. 2006. "A New Class of Highly Dispersed VOx Catalysts on Mesoporous Silica: Synthesis, Characterization, and Catalytic Activity in the Partial Oxidation of Ethanol." Applied Catalysis. A, General 300, no. 2:109-119. PNNL-SA-46146.
Wind R.A., and J. Hu. 2006. "In vivo and ex vivo high-resolution ¹H NMR in biological systems using low-speed magic angle spinning." Progress in Nuclear Magnetic Resonance Spectroscopy 49, no. 3-4:207-259. PNNL-SA-48956.
Wind R.A., J. Hu, and P.D. Majors. 2006. "Localized in Vivo Isotropic-Anisotropic Correlation 1H NMR Spectroscopy Using Ultraslow Magic Angle Spinning." Magnetic Resonance in Medicine 55, no. 1:41-49. PNNL-SA-45789.

2005

Dhamne A., W. Xu, B.G. Fookes, Y. Fan, L. Zhang, S.D. Burton, and J. Hu, et al. 2005. "Polymer-Ceramic Conversion of Liquid Polyaluminasilazanes for SiAlCN Ceramics." Journal of the American Ceramic Society 88, no. 9:2415-2419. PNNL-SA-44828.
Dixon D.A., Z. Dohnalek, M.S. Gutowski, J.Z. Hu, E. Iglesia, B.D. Kay, and J. Liu, et al. 2005. "Early Transition Metal Oxides as Catalysts: Crossing Scales from Clusters to Single Crystals to Functioning Materials." In Frontiers in Catalysis Science: Proceedings of the 12th DOE/BES Heterogeneous Catalysis & Surface Science Meeting, 389-392. Upton, New York:Frontiers in Catalysis Science. PNNL-SA-42058.
Hu J., J. Kwak, J.E. Herrera, Y. Wang, and C.H. Peden. 2005. "Line narrowing in H-1 MAS spectrum of mesoporous silica by removing adsorbed H2O using N-2." Solid State Nuclear Magnetic Resonance 27, no. 3:200-205. PNNL-SA-42819.
Wind R.A., and J. Hu. 2005. "Nuclear Magnetic Resonance Spectroscopy Applications: Proton NMR In Biological Objects Subjected To Magic Angle Spinning." In Encyclopedia of Analytical Science, edited by Paul Worsfold, Alan Townshend, and Colin Poole. 333-342. Amsterdam:Elsevier Academic Press. PNNL-SA-45304.
Wind R.A., H. Bertram, and J. Hu. 2005. "SLOW-MAS NMR METHODS TO STUDY METABOLIC PROCESSES IN VIVO AND IN VITRO." In Magnetic Resonance in Food Science: The Multivariate Challenge, edited by P. S. Belton, S. B. Engelsen, Hans J�rgen Jakobsen. 156-165. New York, New York:Royal Society of Chemistry. PNNL-SA-49849.
Wind R.A., J. Hu, and P.D. Majors. 2005. "Slow-MAS NMR: A New Technology for In Vivo Metabolomic Studies." Drug Discovery Today. Technologies 2, no. 3:291-294. PNNL-SA-45494. doi:10.1016/j.ddtec.2005.08.009

2004

Bertram H., J. Hu, D.N. Rommereim, R.A. Wind, and H.J. Andersen. 2004. "Dynamic High-Resolution H-1 and P-31 NMR Spectroscopy and H-1 T-2 Measurements in Postmortem Rabbit Muscles Using Slow Magic Angle Spinning." Journal of Agricultural and Food Chemistry 52, no. 9:2681-2688. PNNL-SA-41831.
Hu J.Z., R.A. Wind, J.S. Mclean, Y.A. Gorby, C.T. Resch, and J.K. Fredrickson. 2004. "High Resolution 1H NMR Spectroscopy of Metabolically Active Microorganisms Using Non-Destructive Magic Angle Spinning." Spectroscopy 19, no. 12:98-103. PNNL-SA-42335.

2003

Hu J., and R.A. Wind. 2003. "Sensitivity-enhanced Phase Corrected Ultra-slow Magic Angle Turning Using Multiple-Echo Data Acquisition." Journal of Magnetic Resonance 163, no. 1:149-162. PNNL-SA-37766.
Wind R.A., and J. Hu. 2003. "Magnetic susceptibility effects in nuclear magnetic resonance spectroscopy of biological objects." In Recent Research Developments in Magnetism and Magnetic Materials, edited by S.G. Pandalai. 147-169. Trivandrum:Transworld Research Network. PNNL-SA-38967.
Wind R.A., J. Hu, and D.N. Rommereim. 2003. "High Resolution H-1 NMR Spectroscopy in a Live Mouse subjected to 1.5 Hz Magic Angle Spinning." Magnetic Resonance in Medicine 50, no. 6:p. 1113-1119. PNNL-SA-38565.

2002

Barich D.H., J. Hu, R.J. Pugmire, and D.M. Grant. 2002. "Carbon-13 Chemical-Shift Tensors in Polycyclic Aromatic Compounds: Fluoranthene and Decacyclene." Journal of Physical Chemistry A 106. PNNL-SA-45310.
Hu J., and R.A. Wind. 2002. "The evaluation of different MAS techniques at low spinning rates in aqueous samples and in the presence of magnetic susceptibility gradients." Journal of Magnetic Resonance 159, no. 1:92-100. PNNL-SA-37899.
Hu J., D.N. Rommereim, and R.A. Wind. 2002. "High Resolution 1H NMR Spectroscopy in Rat Liver Using Magic Angle Turning at a 1 Hz Spinning Rate." Magnetic Resonance in Medicine 47, no. 5:829-836. PNNL-SA-35454.

2001

Hu J., C.M. Taylor, R.J. Pugmire, and D.M. Grant. 2001. "A Novel Dipolar Dephasing Method for the Slow Magic Angle Turning Experiment." Journal of Magnetic Resonance 152, no. 1:7-13. PNNL-SA-35489. doi:10.1006/jmre.2001.2380
Wind R.A., J. Hu, and D.N. Rommereim. 2001. "High Resolution 1H NMR Spectroscopy in Organs and Tissues Using Slow Magic Angle Spinning." Magnetic Resonance in Medicine 46, no. 2:213-218. PNNL-SA-34181.

2000

Hu J., M.S. Solum, R.A. Wind, B.L. Nilsson, M.A. Peterson, R.J. Pugmire, and D.M. Grant. 2000. "1H and 15N Dynamic Nuclear Polarization Studies of Carbazole." Journal of Physical Chemistry A 104. PNNL-SA-35513.
Wind R.A., B. Shi, J. Hu, M.S. Solum, P.D. Ellis, D.M. Grant, and R.J. Pugmire, et al. 2000. "H-1 Dynamic Nuclear Polarization in Supercritical Ethylene at 1.4 T." Journal of Magnetic Resonance 143, no. 1:233-239. PNNL-SA-32121.

1997

Hu J., J. Zhou, B. Yang, L. Li, J. Qiu, C. Ye, and M.S. Solum, et al. 1997. ""Dynamic Nuclear Polarization of Nitrogen-15 In Benzamide"." Solid State Nuclear Magnetic Resonance 8, no. 2:129-137. PNNL-SA-35523. doi:10.1016/S0926-2040(96)01263-5