The evaluation of different MAS techniques at low spinning rates in aqueous samples and in the presence of magnetic susceptibility gradients

November 1, 2002

Journal Article

The evaluation of different MAS techniques at low spinning rates in aqueous samples and in the presence of magnetic susceptibility gradients

Abstract

It was recently demonstrated that the nuclear magnetic resonance (NMR) linewidths for stationary biological samples are dictated mainly by magnetic susceptibility gradients, and that phase-altered spinning sideband (PASS) and phase-corrected magic angle turning (PHORMAT) solid-state NMR techniques employing slow and ultra-slow magic angle spinning (MAS) frequencies can be used to overcome the static susceptibility broadening to yield high-resolution, spinning sideband (SSB)-free 1H NMR spectra.

Revised: November 10, 2005 | Published: November 1, 2002

Citation

Hu J., and R.A. Wind. 2002. The evaluation of different MAS techniques at low spinning rates in aqueous samples and in the presence of magnetic susceptibility gradients. Journal of Magnetic Resonance 159, no. 1:92-100. PNNL-SA-37899.