March 27, 2017
Report

Characterization of Non-pertechnetate Species Relevant to the Hanford Tank Waste

Abstract

Among radioactive constituents present in the tank waste stored at the U.S. DOE Hanford Site, technetium-99 (Tc), which is generated from the fission of 235U and 239Pu in high yields, presents a unique challenge in that it has a long half-life ( = 292 keV; T1/2 = 2.11105 y) and exists predominately in soluble forms in the liquid supernatant and salt cake fractions of the waste. In the strongly alkaline environments prevalent in most of the tank waste, its dominant chemical form is pertechnetate (TcO4-, oxidation state +7). However, attempts to remove Tc from the Hanford tank waste using ion-exchange processes specific to TcO4- only met with limited success, particularly when processing tank waste samples containing elevated concentrations of organic complexants. This suggests that a significant fraction of the soluble Tc can be present as low-valent Tc (oxidation state

Revised: October 17, 2017 | Published: March 27, 2017

Citation

Chatterjee S., A. Andersen, Y. Du, M.H. Engelhard, G.B. Hall, T.G. Levitskaia, and W.W. Lukens, et al. 2017. Characterization of Non-pertechnetate Species Relevant to the Hanford Tank Waste Richland, WA: Pacific Northwest National Laboratory.