December 4, 2015
Report

Spectroscopic Properties of Tc(I) Tricarbonyl Species Relevant to the Hanford Tank Waste

Abstract

Technetium-99 (Tc) exists predominately in soluble forms in the liquid supernatant and salt cake fractions of the nuclear tank waste stored at the U.S. DOE Hanford Site. In the strongly alkaline environments prevalent in the tank waste, its dominant chemical form is pertechnetate (TcO4-, oxidation state +7). However, attempts to remove Tc from the Hanford tank waste using ion-exchange processes specific to TcO4- only met with limited success, particularly processing tank waste samples containing elevated concentrations of organic complexants. This suggests that a significant fraction of the soluble Tc can be present as non-pertechnetate low-valent Tc (oxidation state

Revised: June 12, 2017 | Published: December 4, 2015

Citation

Levitskaia T.G., A. Andersen, S. Chatterjee, G.B. Hall, E.D. Walter, and N.M. Washton. 2015. Spectroscopic Properties of Tc(I) Tricarbonyl Species Relevant to the Hanford Tank Waste Richland, WA: Pacific Northwest National Laboratory.