On-board storage of hydrogen fuel has been designated as a limiting factor in the advancement of fuel cell technologies in the automotive industry. The use of cryo-compressed Type III pressure vessels presents one option to overcome this barrier. These multi-material vessels will be expected to perform at high pressure and extreme low temperatures, which creates a complex engineering design challenge. Many materials exhibit highly temperature-dependent properties, which must be considered for the efficient design of cryo-compressed pressure vessels. Complicating this issue, mechanical property data at cryogenic temperatures is sparse. This technical paper provides a description of a test apparatus commissioned specifically to help address this shortcoming. A mechanical test frame was retrofitted with a continuous flow cryostat capable to evaluate various mechanical properties throughout a broad temperature range of 25 °C to -269 °C with a load limit of 10 kN. An investigation of the thermomechanical properties of an epoxy resin was carried out as a demonstration.
Published: August 18, 2021
Citation
Merkel D.R., G. Petrossian, D.T. Clelland, and K.L. Simmons. 2020.A Mechanical Test Frame for Property Evaluations at Cryogenic Temperature. In International SAMPE Technical Conference and Exhibition, June 1, 2020, Virtual, Online, 2020-June. Diamond Bar, California:Society for the Advancement of Material and Process Engineering.PNNL-SA-150569.